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The choice of such potentially interfering materials should be based on sound scienti c judgment with a consideration of the interferences that could occur The speci city for an assay and impurity tests should be approached from two angles: 1 When Impurities Are Available The speci city of an assay method is determined by comparing test results from an analysis of sample containing the impurities, degradation products, or placebo ingredients with those obtained from an analysis of samples without the impurities, degradation products, or placebo ingredients For a stability-indicating assay method, degradation peaks need to be resolved from the drug substance However, these impurities do not need to be resolved from each other.

Unfortunately, this is a popular method to extract nonlinear models, because it is also the most practical and traditional from the point of view of both instrumentation and extraction procedure A complete measurement set-up for DC, small-signal and pulsed S-parameter measurement has been demonstrated [63], allowing consistent modelling; however, it is not usually available to modellers and designers..

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For the impurity test, the determination should be established by spiking drug substance or drug product with the appropriate levels of impurities and demonstrating the separation of these impurities individually and/or from other components in the sample matrix Representative chromatograms should be used 2 If Impurities Are Not Available Speci city may be demonstrated by comparing the test results of samples containing impurities or degradation products to a second well-characterized procedure or other validated analytical procedure (orthogonal method) This should include samples stored under relevant stress conditions (light, heat, humidity, acid/base hydrolysis and oxidation) For the assay method, the two results should be compared; for impurity tests, the impurity pro les should be compared Peak homogeneity tests should be performed using PDA or mass spectrometry to show that the analyte chromatographic peak is not attributable to more than one component.

11. Return to the previous view if you zoomed in. Save your drawing. It should look like Figure 15-27.

Figure 2 illustrates the selectivity of a method to resolve known degradation peaks from the parent peak..

H is a Hilbert space if it is complete with respect to this norm. Completeness here means that any Cauchy sequence of elements of the space converges to an element in the space, in the sense that the norm of di erences approaches zero. A Cauchy

contains these templates. Although you can manually browse to the location (Users\username\ AppData\Roaming\Microsoft\Template\Charts), this is an easier way: 1. On the Insert tab, click Chart. 2. In the Insert Chart dialog box, click Manage Templates. The folder location opens in an Explorer window. From here, you can rename or delete les.

Here are a few more items to remember when creating Web graphics: Resolution doesn t matter. Regardless of the Resolution value you enter into the Image Size dialog box, the Web browser displays one image pixel for every screen pixel (unless you specify an alternative image size in your HTML file). All that counts, therefore, is the pixel measurements the number of pixels wide by the number of pixels tall.

2.rrV)f(S) = 2 a v 0 f 0 + 2.rrf05'6

The reason for the effectiveness of this technique is given in the Von Karmen Institute lecture notes (9). 8.1.2.2 Grid For the model of the precalciner, a block structured body fitted grid was developed. The outside surface of the grid is illustrated in Fig. 8.1. One coal inlet is not visible, but it is located directly opposite the coal inlet that is visible on the conical section. It can be seen that the grid in the region of the coal inlet has been refined. The grid refinement was done by the hanging-node method, which divides each hexahedral cell in to eight new hexahedral cells. The cells were refined in the region encompassed by three concentric spheres with coincident centres at the centre of the coal inlet. Thus, three refinement regions can be seen on the

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